Application of atomic fluorescence spectrometry to firearm discharge residues and trace elemental analysis of bullet leads

dc.contributor.advisorVeillon, Claude
dc.contributor.committeeMemberGeanangel, Russell A.
dc.creatorWarkentin, Robert Hunter
dc.date.accessioned2022-06-22T18:28:11Z
dc.date.available2022-06-22T18:28:11Z
dc.date.copyright1975
dc.date.issued1975
dc.description.abstractFlameless Atomic Fluorescence Spectrometry using electrodeless discharge lamps (EDL) has been applied to two areas of interest in forensic science: firearm discharge residues and trace elemental analysis of bullet leads. Evaluations were made on the basis of (1) whether the required resonance line source - EDL - could be made, (2) whether a multielement line source could be prepared for use in a rapid sequential elemental determination of the respective elements, and (3) to compare the results with neutron activation analysis data. The results showed that this technique was not adequately sensitive for detecting Ba and Sb from firearm discharge residues, but that this technique was sensitive enough to determine levels of Sb in bullet leads. Comparison showed that these data were virtually identical to that obtained by neutron activation analysis, and that the two major manufacturers of .22 caliber ammunition had not changed the Sb content of their formulations over the last six years.
dc.description.departmentChemistry, Department of
dc.format.digitalOriginreformatted digital
dc.format.mimetypeapplication/pdf
dc.identifier.other2777717
dc.identifier.urihttps://hdl.handle.net/10657/9830
dc.language.isoen
dc.rightsThis item is protected by copyright but is made available here under a claim of fair use (17 U.S.C. Section 107) for non-profit research and educational purposes. Users of this work assume the responsibility for determining copyright status prior to reusing, publishing, or reproducing this item for purposes other than what is allowed by fair use or other copyright exemptions. Any reuse of this item in excess of fair use or other copyright exemptions requires express permission of the copyright holder.
dc.titleApplication of atomic fluorescence spectrometry to firearm discharge residues and trace elemental analysis of bullet leads
dc.type.dcmiText
dc.type.genreThesis
dcterms.accessRightsThe full text of this item is not available at this time because it contains documents that are presumed to be under copyright and are accessible only to users who have an active CougarNet ID. This item will continue to be made available through interlibrary loan.
thesis.degree.collegeCollege of Arts and Sciences
thesis.degree.departmentChemistry, Department of
thesis.degree.disciplineChemistry
thesis.degree.grantorUniversity of Houston
thesis.degree.levelMasters
thesis.degree.nameMaster of Science

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